Güncel Gönderiler: Makale Koleksiyonu
Toplam kayıt 194, listelenen: 161-180
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Intramolecular Gold-Catalyzed and NaH-Supported Cyclization Reactions of N-Propargyl Indole Derivatives with Pyrazole and Pyrrole Rings: Synthesis of Pyrazolodiazepinoindole, Pyrazolopyrazinoindole, and Pyrrolopyrazinoindole
(American Chemical Society, 2015)Gold-catalyzed and NaH-supported intramolecular cyclization of N-propargyl indole derivatives with pyrazole and pyrrole units attached to indole is described. An efficient route to the synthesis of pyrazolodiazepinoindole, ... -
Bioactive glasses prepared from organic-mediated B-O-P bonded materials
(Elsevier, 2014)In this study, we introduce an alternative route for the synthesis of bioactive borate-phosphate glasses. Glasses with nominal compositions of xNa2O·yB2O3·zP2O 5 (x = 1, 2; y = 1/2; z = 1/2, 3/2) were obtained via melt-quench ... -
Synthesis, spectral characterisation and thermal behaviours of some new p-tert-butylcalix[4]arene and calix[4]arene-esters containing acryloyl groups
(2013)The mono-, di-, tri-, and tetra-acryloyl esters of p-tert-butylcalix [4]arene and calix[4]arene were synthesised by reacting acryloyl chloride with sodium salts of p-tert-butylcalix[4]arene and calix[4]arene in THF. The ... -
The new metal complex templated polyoxoborate(s) (POB(s)) structures. Synthesis, structural characterization, and hydrogen storage capacities
(Elsevier B.V., 2017)The polyoxoborate(s) (POB(s)) structures, including a neutral ligand-metal complex compound as a template, were synthesized and the structural characterizations were performed via single crystal X-ray diffraction, FTIR, ... -
Synthesis of novel Schiff Bases containing acryloyl moiety and the investigation of spectroscopic and electrochemical properties
(Elsevier B.V., 2016)A novel Schiff bases and their acryloyl derivatives were synthesized through the reaction of p-hydroxybenzaldehyde in order of with aniline, p-chloroaniline, p-nitroaniline, p-methylaniline and p-aminobenzoic acid. The ... -
Use of amino acid-based polymeric material for isolation of a protein from poison
(Elsevier B.V., 2017)Melittin is a small protein with 126 amino acid residues which exists in the bee and snake venom. In this study, the Fe(II)-Ni(II) double-salt incorporated poly(2-hydroxyethyl methacrylate-N-methacryloyl-L-aspartic acid), ... -
Study of structural, surface and hydrogen storage properties of boric acid mediated metal (sodium)-organic frameworks
(Elsevier B.V., 2018)Three boric acid mediated metal organic frameworks were synthesized by solution method with using succinic acid, fumaric acid and acetylene dicarboxylic acid as a ligand source and sodium as a metal source. The complexes ... -
Structural, absorption, and molecular properties of o,o'-dihydroxyazo resorcinol dyes bearing an acryloyloxy group
(Elsevier B.V., 2017)To the best of our knowledge, this is the first study reporting the synthesis and characterization of o,o?-dihydroxyazo dyes bearing an acryloyl group. The o,o?-dihydroxyazo dyes were synthesized through coupling of ... -
Fabrication and characterization of magnesium and calcium trimesate complexes via ion-exchange and one-pot self-assembly reaction
(Elsevier B.V., 2018)Using two different synthesis methods, two diversified magnesium and calcium complexes were successfully prepared. When the ion exchange method was used, C9H14MgO11.H2O and C18H30Ca3O24 complexes were obtained. When the ... -
Synthesis and characterization of boric acid mediated metal-organic frameworks based on trimesic acid and terephthalic acid
(Elsevier B.V., 2017)The new metal-organic framework materials based on boric acid reported herein. Sodium and boron containing metal-organic frameworks were synthesized by one-pot self-assembly reaction in the presence of trimesic acid and ... -
Synthesis and characterization of 1,3,4-thiadiazole compounds derived from 4-phenoxybutyric acid for antimicrobial activities
(Elsevier B.V., 2018)New 1,3,4-thiadiazole compounds were synthesized through the cyclization reaction of 4-phenoxybutyric acid and N-phenylthiosemicarbazide derivatives with phosphorous oxychloride. The structures of 1,3,4-thiadiazole compounds ... -
Synthesis of new azo schiff bases of pyrazole derivatives and their spectroscopic and theoretical investigations
(Elsevier B.V., 2018)New pyrazole Schiff bases containing azo groups, 4-((E)-phenyldiazenyl)-3-(4-nitrobenzylidene)-1-phenyl-pyrazole-5-amine and its series, were synthesized using the condensation reaction between p-nitrobenzaldehyde and ... -
Novel mixed ligand complexes of acesulfame / nicotinamide with some transition metals. Synthesis, crystal structural characterization, and biological properties
(Elsevier B.V., 2019)The salt type mixed ligand metal complexes of CoII (I), NiII (II), CuII (III), ZnII (IV) and MnII (V) were synthesized using neutral ligand nicotinamide and anionic ligand acesulfame. The structural characterizations of ... -
Synthesis, characterization, conformational equilibrium and intramolecular hydrogen bond analysis of Novel Azocalix[4]arenes including acryloyl moiety using DFT studies
(Elsevier B.V., 2019)Azocalix[4]arenes were synthesized via diazo-coupling reaction with aniline in 1:1, 1:2, 1:3 and 1:4 molar ratio. Novel Azocalix[4]arenes having Acryloyl moiety were prepared esterification reaction with metallic sodium ... -
Separation and elution order of the enantiomers of some beta-agonists using polysaccharide-based chiral columns and normal phase eluents by high-performance liquid chromatography
(Elsevier B.V., 2016)In this study separation of enantiomers of 8 chiral ?-agonists were studied on 6 polysaccharide-based chiral columns in polar-organic and alcohol-hydrocarbon mobile phases. No separation of enantiomers was observed on any ... -
Solvent effects on pKa values of some substituted sulfonamides in acetonitrile-water binary mixtures by the UV-spectroscopy method
(2009)The examination of the dissociation constants of sulfonamides is essential in drug-design studies and in explaining the biopharmaceutical properties of substances. The dissociation constants of ten common human and veterinary ... -
Determination of dissociation constants of folinic acid (leucovorin), 5-fluorouracil, and irinotecan in hydro-organic media by a spectrophotometry method
(2010)In this study, a multiwavelength spectrophotometry method was used for the determination of the dissociation constants of drugs used for treatment of colorectal cancer, folinic acid (leucovorin), 5-fluorouracil, and ... -
Boric acid complexes with thiamine (vitamin B1) and pyridoxine (vitamin B6)
(2014)Complexation of boric acid with vitamins B1 (thiamine) and B6 (pyridoxine) was investigated. The products were isolated from aqueous solutions and characterized by elemental analysis, FT-IR, 13C MAS NMR and thermal methods. ... -
Boric acid complexes with organic biomolecules: Mono-chelate complexes with salicylic and glucuronic acids
(2010)Two mono-chelate borate complexes, lithium mono-salicylatoborate and sodium mono-glucuronatoborate, are reported for the first time. The complexes were isolated from aqueous solutions and characterized by FTIR (Fourier ... -
A comparative examination of mono- and bis-chelate salicylatoborate complexes and the crystal structure of layered magnesium bis-salicylatoborate
(2011)Complexes of boric acid with sodium- and magnesium-salicylates were prepared and analyzed to examine the structural consequences resulting from the coordination of the salicylate ligand in mono- and bis-chelate modes. The ...
