Güncel Gönderiler: Makale Koleksiyonu
Toplam kayıt 194, listelenen: 141-160
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Structural and thermal studies of non-metal cation pentaborate salts with cations derived from 1,5-diazobicyclo[4.3.0]non-5-ene, 1,8-diazobicyclo[5.4.0] undec-7-ene and 1,8-bis(dimethylamino)naphthalene
(Elsevier B.V., 2012)The reaction of the cyclic amines 1,5-diazobicyclo[4.3.0]non-5-ene (DBN), 1,8-diazobicyclo[5.4.0]undec-7-ene (DBU) and 1,8-bis(dimethylamino)naphthalene (PS) with B(OH)3 in a 1:5 ratio affords in high yields the non-metal ... -
Diphenic acid/nicotinamide and 1,10-phenanthroline complexes of CoII, CuII and ZnII. Synthesis and structural investigation
(Elsevier Ltd, 2016)The complexes of diphenic acid with CoII and CuII metals and diphenic acid/nicotinamide mixed ligand with CoII and ZnII metals were synthesized and characterized of structural properties by elemental analysis, FT-IR spectra, ... -
Fe(II)-Co(II) double salt incorporated magnetic hydrophobic microparticles for invertase adsorption
(Humana Press Inc., 2015)Invertase (β-fructofuranoside fructohydrolase, EC 3.2.1.26) is an enzyme widely used in the food industry. Its main function is the formation of glucose and fructose through hydrolysis of sucrose. For the separation and ... -
Simultaneous determination and validation of emtricitabine, rilpivirine and tenofovir from biological samples using LC and CE methods
(John Wiley and Sons Ltd, 2018)A combination of antiretroviral agents is frequently used in effective treatment of the human immunodeficiency virus infection. In this study, two different separation methods are presented for the simultaneous determination ... -
Spectroscopic and thermal properties of newly mixed azocalix[4]arene ester derivatives
(Elsevier B.V., 2014)The mono-, di-, tri-, and tetra-acryloyl esters of p-chloroazocalix[4]arene which include the first examples of mixed azo ester dyes were synthesized by reacting acryloyl chloride with sodium salts of p-chloroazocalix[4]arene ... -
Determination of pKa values of some sulfonamides by LC and LC-PDA methods in acetonitrile-water binary mixtures
(2010)As constantes de dissociação de sete sulfonamidas antibióticas, sulfadiazina, sulfatiazol, sulfamerazina, sulfametazina, sulfamonometoxina, sulfadoxina e sulfametoxazol, foram determinadas em diferentes misturas binárias ... -
Determination of protonation constants of some tetracycline antibiotics by potentiometry and LC methods in water and acetonitrile-water binary mixtures
(2009)Uma estimativa acurada das constantes de dissociação de antibióticos tetraciclina em misturas binárias acetonitrila-água é muito importante para muitas técnicas de separação, como cromatografia líquida e eletroforese capilar ... -
Determination of dissociation constants of some antifungal drugs by two different methods at 298 K
(2013)The dissociation constants of eight antifungal drugs (fenticonazole, isoconazole, itraconazole, ketoconazole, miconazole, ornidazole, tinidazole, tioconazole) have been determined in water and acetonitrile-water binary ... -
Preparation and characterization of polyvinyl alcohol based copolymers as wound dressing fibers
(Taylor and Francis Inc., 2015)Biocompatible polyvinyl alcohol/polyethylene glycol and polyvinyl alcohol/polypropylene glycol copolymer mats were prepared by electrospinning. The composite fiber mats were subjected to detailed physical analysis complemented ... -
Production of Magnetic Nano-bioconjugates via Ball Milling of Commercial Boron Powder with Biomolecules
(Wiley-VCH Verlag, 2016)Mechanochemical preparation and characterization of surface-functionalized magnetic boron nanoparticles for biomedical applications are presented. Alloying with the stainless steel ball milling material during mechanochemical ... -
Synthesis of pyrrolo-pyrrolo-pyrazines via the Pd/C-catalyzed cyclization of N-propargyl pyrrolinyl-pyrrole derivatives
(Elsevier Ltd, 2019)A novel and efficient synthesis of N-substituted dipyrrolo[1,2-a:2',1'-c]pyrazine derivatives has been developed. The synthetic strategy relies on the synthesisof 4',5'-dihydro-1H,3'H-2,2'-bipyrrole, followed by the reaction ... -
Synthesis of a bipyridine-derived achiral thiourea trifluoromethanesulfonic acid salt and its application as an additive in organocatalytic asymmetric reactions
(2013)The host-guest complex of a proline-thiourea bipyridine trifluoromethanesulfonic acid salt can catalyze organocatalytic asymmetric reactions such as aldol, Michael, and Mannich in polar protic medium with high stereoselectivities. ... -
Determination of pKa values of some antihypertensive drugs by liquid chromatography and simultaneous assay of lercanidipine and enalapril in their binary mixtures
(Elsevier B.V., 2010)In this study, pKa values were determined using the dependence of the retention factor on the pH of the mobile phase for three ionizable substances, namely, enalapril, lercanidipine and ramipril (IS). The effect of the ... -
Electroanalytical characteristics of antipsychotic drug ziprasidone and its determination in pharmaceuticals and serum samples on solid electrodes
(Elsevier B.V., 2010)Ziprasidone is a psychotropic agent used for the treatment of schizophrenia. Its oxidation was investigated electrochemically at boron-doped diamond and glassy carbon electrodes using cyclic, differential pulse, and square ... -
Analytical application of polymethylene blue-multiwalled carbon nanotubes modified glassy carbon electrode on anticancer drug irinotecan and determination of its ionization constant value
(Elsevier B.V., 2013)The voltammetric behavior of anticancer drug irinotecan (IRT) was investigated at poly (methylene blue)/multi-walled carbon nanotube (PMB/MWCNT) modified glassy carbon electrode (GCE). The modified electrode surface was ... -
Electrochemical preparation of sodium dodecylsulfate doped over-oxidized polypyrrole/multi-walled carbon nanotube composite on glassy carbon electrode and its application on sensitive and selective determination of anticancer drug: Pemetrexed
(Elsevier B.V., 2014)Electrochemical oxidation of pemetrexed (PMX) was studied on bare, carboxylic acid functionalized multi-walled carbon nanotubes and over-oxidized polypyrrole modified (oo-PPy/MWCNTs-COOH/GCE) glassy carbon electrodes by ... -
Investigation of voltammetric behavior and electroanalytical determination of anticancer epirubicin via glassy carbon electrode using differential pulse and square wave voltammetry techniques
(Editions de l'Academie Republique Populaire, 2015)The electrochemical oxidation of epirubicin was investigated using cyclic, differential pulse and square wave voltammetry at glassy carbon electrode. The aim of the study was to determine epirubicin levels in pharmaceuticals ... -
Boric acid: A simple molecule of physiologic, therapeutic and prebiotic significance
(Walter de Gruyter GmbH, 2015)Boric acid, H3BO3, is a weak acid and at physiological pH is in the form of an uncharged small molecule. Behaving as a Lewis acid, it forms complexes with amino- and hydroxy acids, carbohydrates, nucleotides and vitamins ... -
Synthesis, characterization of poly-2- (2-hydroxybenzylideneamino)-6- phenyl-4,5,6, 7-tetrahydrobenzo[b]thiophene-3-carbonitrile: Investigation of antibacterial activity and optical properties
(2012)The oxidative polycondensation reaction conditions of 2-(2- hydroxybenzylideneamino)-6-phenyl-4,5,6,7-tetrahydrobenzo[b]thiophene-3- carbonitrile were examined. The magnitude of the reflectance of the polymer decreases ... -
Design of pyrazolo-pyrrolo-pyrazines and pyrazolo-pyrrolo-diazepines via AuCl3-catalyzed and NaH-supported cyclization of N -propargyl pyrazoles
(American Chemical Society, 2015)A concise synthetic methodology for new heterocyclic scaffolds, such as pyrazolo-pyrrolo-pyrazine and pyrazolo-pyrrolo-diazepine skeletons, was developed. The key features of this method include (i) synthesis of pyrrole-derived ...
