Güncel Gönderiler: Fen Edebiyat Fakültesi
Toplam kayıt 674, listelenen: 601-620
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Design of pyrazolo-pyrrolo-pyrazines and pyrazolo-pyrrolo-diazepines via AuCl3-catalyzed and NaH-supported cyclization of N -propargyl pyrazoles
(American Chemical Society, 2015)A concise synthetic methodology for new heterocyclic scaffolds, such as pyrazolo-pyrrolo-pyrazine and pyrazolo-pyrrolo-diazepine skeletons, was developed. The key features of this method include (i) synthesis of pyrrole-derived ... -
Intramolecular Gold-Catalyzed and NaH-Supported Cyclization Reactions of N-Propargyl Indole Derivatives with Pyrazole and Pyrrole Rings: Synthesis of Pyrazolodiazepinoindole, Pyrazolopyrazinoindole, and Pyrrolopyrazinoindole
(American Chemical Society, 2015)Gold-catalyzed and NaH-supported intramolecular cyclization of N-propargyl indole derivatives with pyrazole and pyrrole units attached to indole is described. An efficient route to the synthesis of pyrazolodiazepinoindole, ... -
Bioactive glasses prepared from organic-mediated B-O-P bonded materials
(Elsevier, 2014)In this study, we introduce an alternative route for the synthesis of bioactive borate-phosphate glasses. Glasses with nominal compositions of xNa2O·yB2O3·zP2O 5 (x = 1, 2; y = 1/2; z = 1/2, 3/2) were obtained via melt-quench ... -
Synthesis, spectral characterisation and thermal behaviours of some new p-tert-butylcalix[4]arene and calix[4]arene-esters containing acryloyl groups
(2013)The mono-, di-, tri-, and tetra-acryloyl esters of p-tert-butylcalix [4]arene and calix[4]arene were synthesised by reacting acryloyl chloride with sodium salts of p-tert-butylcalix[4]arene and calix[4]arene in THF. The ... -
The new metal complex templated polyoxoborate(s) (POB(s)) structures. Synthesis, structural characterization, and hydrogen storage capacities
(Elsevier B.V., 2017)The polyoxoborate(s) (POB(s)) structures, including a neutral ligand-metal complex compound as a template, were synthesized and the structural characterizations were performed via single crystal X-ray diffraction, FTIR, ... -
Synthesis of novel Schiff Bases containing acryloyl moiety and the investigation of spectroscopic and electrochemical properties
(Elsevier B.V., 2016)A novel Schiff bases and their acryloyl derivatives were synthesized through the reaction of p-hydroxybenzaldehyde in order of with aniline, p-chloroaniline, p-nitroaniline, p-methylaniline and p-aminobenzoic acid. The ... -
Use of amino acid-based polymeric material for isolation of a protein from poison
(Elsevier B.V., 2017)Melittin is a small protein with 126 amino acid residues which exists in the bee and snake venom. In this study, the Fe(II)-Ni(II) double-salt incorporated poly(2-hydroxyethyl methacrylate-N-methacryloyl-L-aspartic acid), ... -
Study of structural, surface and hydrogen storage properties of boric acid mediated metal (sodium)-organic frameworks
(Elsevier B.V., 2018)Three boric acid mediated metal organic frameworks were synthesized by solution method with using succinic acid, fumaric acid and acetylene dicarboxylic acid as a ligand source and sodium as a metal source. The complexes ... -
Structural, absorption, and molecular properties of o,o'-dihydroxyazo resorcinol dyes bearing an acryloyloxy group
(Elsevier B.V., 2017)To the best of our knowledge, this is the first study reporting the synthesis and characterization of o,o?-dihydroxyazo dyes bearing an acryloyl group. The o,o?-dihydroxyazo dyes were synthesized through coupling of ... -
Fabrication and characterization of magnesium and calcium trimesate complexes via ion-exchange and one-pot self-assembly reaction
(Elsevier B.V., 2018)Using two different synthesis methods, two diversified magnesium and calcium complexes were successfully prepared. When the ion exchange method was used, C9H14MgO11.H2O and C18H30Ca3O24 complexes were obtained. When the ... -
Synthesis and characterization of boric acid mediated metal-organic frameworks based on trimesic acid and terephthalic acid
(Elsevier B.V., 2017)The new metal-organic framework materials based on boric acid reported herein. Sodium and boron containing metal-organic frameworks were synthesized by one-pot self-assembly reaction in the presence of trimesic acid and ... -
Synthesis and characterization of 1,3,4-thiadiazole compounds derived from 4-phenoxybutyric acid for antimicrobial activities
(Elsevier B.V., 2018)New 1,3,4-thiadiazole compounds were synthesized through the cyclization reaction of 4-phenoxybutyric acid and N-phenylthiosemicarbazide derivatives with phosphorous oxychloride. The structures of 1,3,4-thiadiazole compounds ... -
Synthesis of new azo schiff bases of pyrazole derivatives and their spectroscopic and theoretical investigations
(Elsevier B.V., 2018)New pyrazole Schiff bases containing azo groups, 4-((E)-phenyldiazenyl)-3-(4-nitrobenzylidene)-1-phenyl-pyrazole-5-amine and its series, were synthesized using the condensation reaction between p-nitrobenzaldehyde and ... -
Novel mixed ligand complexes of acesulfame / nicotinamide with some transition metals. Synthesis, crystal structural characterization, and biological properties
(Elsevier B.V., 2019)The salt type mixed ligand metal complexes of CoII (I), NiII (II), CuII (III), ZnII (IV) and MnII (V) were synthesized using neutral ligand nicotinamide and anionic ligand acesulfame. The structural characterizations of ... -
The effect of alloying element Zn on magnetic properties of martensite phase in FeNiMn alloy
(Elsevier B.V., 2018)The effect of alloying element Zn on the characteristics of thermal induced martensite and magnetic properties of martensite phase were investigated with scanning electron microscopy (SEM) and Mössbauer spectroscopy ... -
Restricted rotation around the methylene bridge of 5-(2-p-(chlorophenyl)benzimidazole-1-yl)methyl-4-(o-substitutedphenyl)-2,4-dihydro-[1,2,4]-triazole-3-thiones as evidenced by NMR, X-RAY and DFT studies and the importance of low energy rotational conformers
(Elsevier B.V., 2019)The aim of this study was to clarify the restricted rotation around the –CH2–N bond of the compounds, 5-(2-(p-chlorophenylbenzimidazol-1-yl-methyl)-4-(o-methylphenyl)-2,4-dihydro-[1,2,4]-triazole-3 thione [1], 4-(o-florophenyl)- ... -
Synthesis, characterization, conformational equilibrium and intramolecular hydrogen bond analysis of Novel Azocalix[4]arenes including acryloyl moiety using DFT studies
(Elsevier B.V., 2019)Azocalix[4]arenes were synthesized via diazo-coupling reaction with aniline in 1:1, 1:2, 1:3 and 1:4 molar ratio. Novel Azocalix[4]arenes having Acryloyl moiety were prepared esterification reaction with metallic sodium ... -
Temperature lag effect on TL glow peaks: Corrections on kinetic parameters
(Elsevier B.V., 2018)Analyses on TL glow curves recorded with various heating rates for some ternary and quaternary crystals were accomplished using peak maximum temperatures (Tmax) which are experimentally obtained and corrected according to ... -
The effect of austenitizing time on martensite morphologies and magnetic properties of martensite in Fe-24.5%Ni-4.5%Si alloy
(2007)The effect of austenitizing time on the formation of martensite in Fe-24.5%Ni-4.5%Si alloy has been studied by means of transmission electronmicroscope (TEM), scanning electronmicroscope (SEM) and Mössbauer spectroscopy ... -
Investigation of the time evolution of Lane-emden-type Kanai-caldirola oscillator
(2009)In this study, we have investigated the time evolution of the first kind Lane-Emden-type Kanai-Caldirola oscillator. The total energy of the one dimensional classical harmonic oscillator with time-dependent mass is obtained. ...
